- Research article
- Open Access
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# Design of an enhanced mechanism for a new Kibble balance directly traceable to the quantum SI

*EPJ Techniques and Instrumentation*
**volume 9**, Article number: 7 (2022)

## Abstract

The “Quantum Electro-Mechanical Metrology Suite” (QEMMS) is being designed and built at the National Institute of Standards and Technology. It includes a Kibble balance, a graphene quantum Hall resistance array and a Josephson voltage system, so that it is a new primary standard for the unit of mass, the kilogram, directly traceable to the International System of Units (SI) based on quantum constants. We are targeting a measurement range of 10 g to 200 g and optimize the design for a relative combined uncertainty of \(2\times 10^{-8}\) for masses of 100 g. QEMMS will be developed as an open hardware and software design. In this article, we focus on the design of an enhanced moving and weighing mechanism for the QEMMS based on flexure pivots.

## Introduction

The Kibble balance is the instrument for the precise primary realization of the unit of mass in the International System of Units (SI) based on electro-mechanical metrology principles and quantum physics. Due to the design of a new version of the Kibble balance at the National Institute of Standards and Technology (NIST) as part of the so-called “Quantum Electro-Mechanical Metrology Suite”, QEMMS, this article describes the components integrated in QEMMS as well as the design of the new flexure-based moving and weighing mechanism.

## The Kibble balance

The measuring principle of the Kibble balance was invented in 1976 by the metrologist Dr. Bryan Kibble at the National Physical Laboratory of the United Kingdom [1]. It was one of the main experiments contributing to the redefinition of the SI in the year 2018 [2, 3]. The redefinition of the unit of mass, the kilogram, based on the fixed values of three constants of nature—the Planck’s constant, *h*, the speed of light, *c*, and the hyperfine transition frequency of Caesium, \(\Delta \nu _{\text{Cs}}\)—provides a means to realize mass through electrical metrology using absolute precision balances without the need to compare to a physical object.

Until 2018, only the values for *c* and \(\Delta \nu _{\text{Cs}}\) were fixed, and the International Prototype Kilogram (IPK) was the last physical artifact defining one of the seven SI base units. Using the Kibble balance principle and decades of hard work, scientists were able to measure and define a numerical value for *h* based on the mass of the IPK, the speed of light and the hyperfine transition frequency of Caesium. As a result, the Kibble balance can be operated in a reversed fashion and realize virtually any macroscopic mass value directly from the defined value of *h*. A visualization of this relation is shown in Fig. 1.

The Kibble balance uses two modes of operation for an absolute mass measurement. In the first one, the weighing mode, the gravitational force of a test mass is directly compensated by a counter force such that the test mass stays at a defined null position. The counter force is provided by a magnet-coil system and can be controlled by adjusting the current through the coil, see Fig. 2.

The equation for this mode of operation is

where *m* is the mass of the test mass, *g* the local gravitational acceleration, *N* the number of turns of the wire in the coil, Φ the magnetic flux through the coil, *z* the position of the coil along the vertical direction, and *I* the electric current through the coil.

Since the magnetic flux gradient \(N \partial \Phi / \partial z\) is very hard to obtain with sufficient uncertainty, a second mode of operation, the velocity mode, allows for direct measurement of the \(N \partial \Phi / \partial z\) with the required precision. Here, the coil is moved up and down in the magnetic field of the magnet such that a voltage is induced in the coil. Derived from Faraday’s induction law it yields,

where *V* is the voltage induced in the coil in the velocity mode, and *v* is the vertical velocity of the coil with respect to the magnet, see Fig. 3. The velocity in high precision Kibble balances is usually measured with an interferometer and vacuum operation of the balance creates an environment with a stable index of refraction. Solving both equation (1), and equation (2) for \(N \partial \Phi / \partial z\) and equating them yields

On the left hand side in equation (3), we see the expression for mechanical power, and on the right hand side, the one for electrical power. The original name of the Kibble balance, “watt balance”, is a reflection of the power balance principle described here.

A direct measurement of mass traceable to the new SI as in the QEMMS would not be possible without two quantum effects: The Josephson effect and the quantum Hall effect. The electric current *I* through the coil in the weighing mode is usually measured according to Ohm’s law by monitoring a voltage drop over a traditional resistor *R* with very precisely known value (see Fig. 2), which is calibrated against a quantum Hall resistor (QHR) standard \(R_{\mathrm{H}} = h/(i e^{2})\) where *i* is the Landau level filling factor [4, 5] and *e* is the elementary charge. A Programmable Josephson Voltage System (PJVS) is a frequency to voltage converter, that is, \(V=\nu /K_{J}\) where \(K_{J}=2e/h\) [6] and *ν* is a frequency. The PJVS provides a primary realization for voltage and is put parallel to the resistor in the electric circuit. It is used to create a voltage nominally equal to the drop over the resistor and a calibrated voltmeter monitors the remaining potential difference in the circuit. The voltage, hence, appears in the weighing mode, and the velocity mode. Adding the Josephson and quantum Hall effect to equation (3) yields the link of mass with Planck’s constant established with the Kibble balance:

Furthermore, the velocity and the local gravitational acceleration in equation (4) are measured using primary standards of length and time based on the definition of the second and meter traceable to \(\Delta \nu _{\text{Cs}}\) and *c*, respectively.

More detailed information on the link of the quantum effects with the Kibble balance equation can be found in [7, 8].

## The QEMMS

There are multiple Kibble balance experiments around the globe. The design of each Kibble balance is unique, however, one feature seems to be common to all: The resistor in the electrical circuit for the weighing mode (see Fig. 2) is calibrated using transfer standards against a QHR as primary standard for resistance. QEMMS will overcome the inconvenience of external resistor calibration and thus eliminate the resistance calibration uncertainty by implementing a QHR directly in the Kibble balance’s electrical circuit. This QHR is based on the quantization effect of monolayer graphene [9]. Among the advantages offered by graphene-based QHR standards is their ability to maintain the fully quantized state at higher currents and temperature. NIST researchers fabricated thirteen single element graphene QHR standards in parallel and operate at the Landau level \(i = 2\) plateau, giving a nominal value of \(R_{\mathrm{K}}/26 \approx {992.8}\ \Omega\) [10]. Even though the graphene QHR array in Panna *et al.* show experiments with maximum currents up to 0.3 mA, measurements have already been published showing single Hall bar graphene devices maintaining quantization for currents up to 0.7 mA [11]. Furthermore, creating arrays with higher currents is subject to extensive research efforts at NIST. In context of QEMMS, these allow for a measurement of masses up to 200 g, depending on the design of the coil in the magnetic field [12].

Hence, this will be the first integrated instrument in the world to feature all three: a Kibble balance for the actual mass measurement, a PJVS, and a primary reference resistor directly implemented in the instrument, which provides an outlook for improved overall measurement uncertainty for masses. The entire QEMMS will fit in one room of the size of approximately \({4}~\mathrm{m} \times {5}~\mathrm{m}\) (width × length). Through the direct link to all three natural constants *h*, *c* and \(\Delta \nu _{\text{Cs}}\), it is providing direct SI realization for the units of mass, time, length, electrical resistance, voltage, and current. Thus, the QEMMS can be seen as a metrology institute in one single experiment.

As opposed to traditional Kibble balances [8] which were designed and optimized to measure 1 kg, the QEMMS is being built to cover a mass range of \({10}~\mbox{g}\) to \({200}~\mbox{g}\). We optimize the design specifically targeting a relative combined measurement uncertainty of \(2\times 10^{-8}\) at nominal mass value of 100 g. Here, we want to take advantage of the direct implementation of the new quantum SI in the instrument for mass scaling. A factor of 20 in the total mass range has proven convenient for systematic studies on the balance, which motivates the covered range around the nominal value. Furthermore, smaller nominal mass values allow for a more robust and compact design, which makes the technology more accessible for other metrology institutes as well.

Since a QHR has been designed for this purpose [10], we put the focus on the redesign and optimization of the Kibble balance. Each individual subsystem of the Kibble balance is being investigated regarding new opportunities for improvement. The permanent magnet system [12] and a vacuum chamber [13] have already been acquired. In the current design step, improvement of the mechanical components in the balance, especially the mechanism, is of key interest since the state of the art seems to be one of the limiting factors for the overall balance uncertainty. Hence, the design of the QEMMS mechanism is the focus of the following chapters.

### Requirements to the QEMMS mechanism

The mechanism in the QEMMS has two functions: It provides suspension and defines the trajectory of moving components. The former entails suspending all functional components of the balance such as the mass pan, the coil, a counterweight for balancing, the coil suspension and optics for the interferometer. The latter requires the mechanism to move the coil in a vertical trajectory through the magnet in velocity mode. We are seeking to integrate these two main functions in the same mechanism so that one mechanical system is used to perform both modes of operation in the QEMMS.

A set of important requirements pre-define a successful mechanism design. The most important aspects that can directly be impacted by conceptual decisions in an early state of design are listed in Table 1.

In general, it is important to keep all uncertainty contributions of the mechanical system to the measurement sufficiently small that their combination does not exceed the targeted uncertainty. For the QEMMS we define this as on the order of parts in 10^{9}. In the following, each requirement from Table 1 is explained in more detail regarding the background of its origin and importance.

#### Coil travel in the velocity mode

For a measurement of \(N \partial \Phi / \partial z\) in the velocity mode, the coil will be moved up and down in the magnetic field of the permanent magnet for the QEMMS. At first, it is accelerated to a velocity of \(v_{\mathrm{z}}={2}~\mathrm{mm}\,\mathrm{s}^{-1}\). Then it will travel with constant speed for 40 mm. Finally, the coil is decelerated to a stop at the end of each sweep. The permanent magnet for the QEMMS has been designed and built to provide uniform \(\partial \Phi / \partial z\) profile over the course of the travel with constant speed. This area is referred to as the precision air gap. [12]

Hence, the travel range of the coil is given by the length of the precision air gap plus additional travel for acceleration and deceleration of the coil. A conservative estimate of the total travel length based on experience with previous Kibble balance designs is \({60}~\mathrm{mm}\). We will use this number as an input parameter for the mechanism design of QEMMS.

#### Stiffness

To keep measurement errors at the necessary minimum and to achieve the required resolution, the balance mechanism needs to have a low stiffness. More importantly, we want the stiffness to be constant in time and over all possible coil positions for the following three reasons:

(a) The noise in the balance position feedback converts to force noise by multiplying the position noise with the stiffness of the mechanism. Hence, a low stiffness produces a small force noise at a stable position which reduces averaging time. Since QEMMS will be optimized to measure 100 g mass artifacts with an overall relative standard uncertainty of \(2\times 10^{-8}\), we are aiming for a resolution of the balance of \(1\times 10^{-9}\) on 100 g. This yields an absolute mass resolution of 0.1 μg, which is roughly equivalent to a force resolution of 1 nN. We assume we can average the position feedback uncertainty down to 100 nm, which means that the mechanism needs to have a stiffness of \(\leq {0.01}~\mathrm{Nm}^{-1}\) at the weighing position to be within the resolution requirements.

(b) A constant stiffness value along the coil travel is important for an accurate and stable feedback control during the velocity mode. A higher order stiffness term causes the balance to become unstable or stiffen up along the travel if the stiffness at the weighing position, which is in the middle of the coil travel, is adjusted down to 0.

(c) The stiffness needs to be constant with time, because changes over time result in a change in the restoring force of the mechanism, which leads to a drifting equilibrium position of the balance and therefore drift in the force signal, which might be limiting for the balance performance.

At present, we are confident that a mechanism stiffness of \(\leq {0.01}~\mathrm{Nm}^{-1}\) will satisfy the above requirements. Experimental validation will follow in the near future. Optionally, we include a stiffness adjustment unit. This can be realized by applying a negative stiffness to the mechanism by means of, e.g., an inverted pendulum, astatic stiffness adjustment, or a negative spring restoring torque [14–16].

#### Guiding of the coil

For QEMMS, the maximum horizontal parasitic motion along the vertical coil travel is 10 μm. Furthermore, we are seeking to create a trajectory with the QEMMS mechanism that is repeatable between weighing and velocity mode as well as between each sweep in the velocity mode.

The coil speed in the velocity mode is measured with a heterodyne interferometer reflecting a laser beam off of a retroreflector that is attached to the moving coil (see Fig. 3). The most basic criterion to run a measurement in the velocity mode is that the interference detector does not lose the beam signal in the sweeping phase. The laser beam of the interferometer needs to be fully reflected. Horizontal displacements and imperfections of the trajectory from the vertical can cause the beam to be clipped. However, before clipping the beam, other impacts to the measurement occur due to imperfections in the coil trajectory from the vertical [17, 18]. Limiting the explanations to the *x*-direction, these are proportional to the term \(v_{\mathrm{x}}/v_{\mathrm{z}}\), where \(v_{\mathrm{x}}\) is a horizontal and \(v_{\mathrm{z}}\) is the vertical coil velocity. In Appendix A, we discuss three biases that occur with horizontal motion. For all, the figure of merit is \(v_{\mathrm{x}}/v_{\mathrm{z}}=\Delta x/\Delta z\approx {1.67\times 10^{-4}}\).

#### Low hysteretic force

Non-linearities from mechanical hysteresis can be a problem in Kibble balances. If hysteresis is too large, then a precise measurement cannot be done because the this is a limitation in the resolution of the balance.

The magnitude of a hysteretic force in general, depends on the load to the pivots and on excitations of the balance, e.g., due to a response of the balance during a mass transfer or the mechanism movement during the velocity mode. There are two general ways to reduce hysteretic forces in balances: (1) Minimizing the excursion during mass placement by adjusting mass lift speed and by optimizing feedback control. (2) Using an erasing procedure where the center pivot point is exercised in a damped sinusoidal motion after each excursion of the balance. However, a small part of hysteresis remains in the system. The goal is to have a remaining hysteretic loss in the mechanism equivalent to ≤ 0.1 μg.

The cause and magnitude of a hysteretic force is also driven by the type of mechanism used in the balance. All balance mechanisms can be divided based on their type of center pivot into two groups: knife edge-based and flexure pivot-based balances. In the QEMMS mechanism, flexure pivots will be employed.

The main advantage of a flexure over a knife edge with regards to hysteresis is that in the flexure only elastic deformation contributes to this effect, whereas in a knife edge elastic and plastic deformation need to be considered. After a change in the load and a deflection, a flexure shows anelastic behavior because it takes time to relax back to its internal equilibrium state. However, despite the similarities to the knife edge, the hysteretic forces in a flexure are known to be smaller. Reviewing literature, T. Quinn [19] published results for a 1 kg mass comparator stating that a flexure-based balance performs mass measurements with precision of up to six orders of magnitude better than a knife edge-based balance. Note that he admits that the knife edge-based balance was probably not ultimately optimized in terms of knife and flat materials and geometry [19–21].

Note also that all published anelasticity data concerning flexures in precision balances were gathered using mass comparators which only use the weighing mode. The anelastic characteristic of flexures was never shown in Kibble balances where the weighing and the velocity mode are both performed by a single flexure mechanism. Conducting a series of experiments is necessary to learn about this effect because it cannot be quantitatively pre-determined during the design process. Unfortunately, theoretical calculation or simulation cannot provide quantitative knowledge regarding hysteretic forces because theories on this topic are not very well developed or validated. There are only general design recommendations that can be applied for minimizing the amount of anelasticity in flexures, for example: (1) designing the flexure as thin as possible in the region of bending, (2) designing it long and (3) using a flexure material with low internal damping coefficient. These recommendations minimize the geometric and elastic part of the stiffness, the internal material friction and therefore the energy stored and dissipated in the flexure during deflection, which is a measure for low hysteresis according to Speake [21].

#### Carrying capacity and installation space

The central pivot in the QEMMS mechanism needs to support a total load of 15 kg. Furthermore, with this load it must be capable of rotating by \(\pm 7\,{}^{\circ}\) to provide the desired \(\pm {30}~\mathrm{mm}\) of vertical travel, assuming the maximum dimension of a beam/wheel limited by the maximum installation space in QEMMS. Since the Kibble balance in QEMMS is designed to be similar in size to commercial high precision vacuum mass comparators, we allow for a maximum horizontal dimension of the mechanism of \(\approx {500}~\mathrm{mm}\). This limits the maximum dimension of one beam or wheel arm in the balance to 250 mm considering symmetric balance design. Also, the mechanism itself needs to be as compact as possible to keep free space for optical systems and a mass exchange unit in the vacuum chamber. The sensitivity of a balance scales as the square of the balance arm [16]. Hence it should be as large as is practically allowed.

Figure 4 visualizes the above explained requirements in a drawing.

### Design of the QEMMS mechanism

We are quite confident that a flexure-based mechanism design keeps the mechanical hysteresis in the QEMMS mechanism small and provides a repeatable movement. Furthermore, the new mechanism should be more compact, lighter, and require less auxiliary control features to define a one-dimensional coil trajectory than existing versions of Kibble balance mechanisms. Henceforth, we favor passive mechanical components built from flexure elements for defining the balance trajectory over auxiliary electrical components. Figure 5 shows the separation of the QEMMS mechanism function in two sub-components integrated in a single mechanical system. One component is for balancing, the other one for defining a linear trajectory of the coil.

We will take a look into how to realize each functional component in Fig. 5 with a flexure design and integrate them into a mechanism that satisfies the requirements for the QEMMS.

#### Main flexure

The trade-off in the design of the main flexure is to keep the maximum stress in the flexure at the maximum deflection angle at an acceptable level. A safety factor of 2 to 3 is desired. Also, a low elastic flexure stiffness is recommended in order to reduce the anelastic effect in the flexure after deflection [21]. This calls for a flexure as thin as possible.

Furthermore, a material with low internal damping/anelasticity must be used in order to avoid hysteretic effects upfront as much as possible. A metal with very high yield strength (\(\approx {1000}~{\mathrm{MPa}}\)) and small anelastic after effect is a hardened Copper Beryllium alloy as used for flexures in balance experiments, e.g., in [19].

These materials are typically machined using wire electrical discharge machining, grinding, high speed milling or etching. In notch flexures, minimal flexure thicknesses of ≈ 50 μm can be achieved.

The main flexure needs to be carefully designed and analyzed by means of finite element analysis in order to evaluate stress-reducing parameters in the flexure accurately. One key factor to evaluate is the stress concentration near axis of rotation of the flexure due to the high axial load and high deflection. Widely used hinge geometries such as flat or conventional circular hinges have limitations for application in the QEMMS because they show high stress values derived from the simulations in Fig. 6. Maximum equivalent stresses of \(>{1000}~{\mathrm{MPa}}\) exceed the static yield strength for the high strength flexure material we chose (\(\approx {1000}~{\mathrm{MPa}}\)).

In the investigated conventional flexure geometries, the bending radius is very small, which causes a high stress concentration in the region of flexing. Thus, we explore a modified flexure geometry that causes the bending radius of the flexure to become larger. This shows a positive effect to the maximum equivalent stress in the flexure. A representation for the modified geometry with an acceptable maximum stress value is shown in Fig. 7.

Figure 8 only represents one set of parameters for a flexure suitable for the application in the QEMMS mechanism. Other variations are possible, but further elaboration on this matter is not within the scope of this manuscript. The optimization of the geometry not only regarding the stress in the flexure but also the elastic stiffness is work in progress at NIST and will be published in a later on.

#### Kinematics

In addition to the main pivot, a sub-mechanism for guiding with a proper link to the main flexure completes the kinematics of the balance. Examples, where a guiding mechanism is combined and linked with a balance beam can be found in, e.g., commercial weighing cells or in the Planck balance at Physikalisch-Technische Bundesanstalt (PTB) [22]. An approach for an integrated design of main flexure and guiding mechanism in a parallel four bar linkage was used at NIST for electrostatic force balance experiments [16, 23]. The mechanisms in [16, 22, 23] show a systematic arc motion caused by the use of a parallel four bar linkage for guiding and use only small travel ranges on the order of micro meters during operation. Thus, these concepts can inspire a new design, but may not be directly used in the QEMMS due to the requirement for purely vertical motion of the coil over a relatively large travel. Other options for building flexure-based guiding mechanisms providing a linear motion need to be explored.

Since a single flexure hinge is always a rotating pivot, only a chain of multiple hinges can provide a (nearly) linear motion of a moving member. An overview and further references to useful literature about principles to combine a series of rotational pivots are provided in [24]. The dissertation thesis addresses the correction of unwanted parasitic motions as well as the change of the degree of freedom in a kinematic structure in order to achieve a certain trajectory. Such principles are, e.g., the design of parallel or serial kinematic structures, or applying nested or external linkage structures to avoid under-constraint in a mechanism [25]. An example based on a planar parallelogram linkage is provided in Fig. 11 in Appendix B.

However, due to simplicity, correction of lateral error motions, compactness, and the convenience in machining of a planar flexure mechanism, we favor the folded parallelogram linkage as a guiding mechanism for the QEMMS. We will integrate a weighing beam/wheel as the external linkage as shown in option (4.2) in Fig. 11 (Appendix B) and use this directly as a link to the main flexure. A visualization of the kinematic system for the QEMMS mechanism is shown in Fig. 9.

In a next step, a comparison of using a beam balance versus a wheel balance is addressed.

#### Beam balance vs. wheel balance

There is a fundamental difference between the kinematics of the two balance types. The end points of the beam balance perform a rotational motion along a fixed circle. Only by the use of a further guiding mechanism, the movement of suspended components can take place parallel to the vector of gravity as shown in Fig. 12 (Appendix C).

In contrast, with the wheel balance, a rolling of a band on the wheel is performed. This results, in theory, in a direct conversion of a rotational movement of the wheel into a linear displacement of suspended components parallel to the vector of the gravitational force. In order to achieve a further improvement in the quality of the linear motion and to avoid unwanted oscillations, a guiding mechanism as shown in Fig. 9 can be used. The resulting overconstrained design can be dealt with by adjustment.

At first glance, this difference in use of a beam to a wheel balance seems to be negligible for application in a balance. Indeed, in a mass comparator, where the mechanism operates closely around its defined zero position, there is no theoretical functional advantage to either solution. All parasitic effects in the kinematics are small due to small deflections of the flexures. Convenience in machining and assembling of small planar (sometimes monolithic) mechanisms seems to be causing the favor for beam balances here.

However, with the large travel required in the QEMMS, not all of the usually negligible effects in the mechanism remain harmless to the mechanical properties of the instrument. In fact, there is one impact that causes a major disadvantage of a beam balance compared to a wheel balance from a kinetic perspective: there is a horizontal force acting upon the connecting links between the guiding mechanism and the beam when the effective horizontal length of the balance beam shortens by the cosine of the deflection angle.

This results in a non-linear stiffness term and parasitic forces to the guiding mechanism which cause unwanted deformations and error motions in the guide. An analysis of this effect is provided Appendix C.

We could think of compensating the parasitic horizontal force on the stages by applying a symmetric compensation design approach by adding more components to a beam balance-based mechanism. However, this would increase the complexity of the mechanism to a level that we do not desire. The fact that the wheel balance prevents this horizontal force by design causes a favor of the wheel over the beam balance for the QEMMS mechanism.

#### Modular design

The mechanism has been designed based on a wheel balance and a rendering of the frame and the moving parts can be seen in Fig. 10. We favor a prototype of modular build to allow for variation of single components in experiments. Interesting elements for variation would be, e.g., the main flexure or the guiding mechanism flexures with view on the hysteretic properties of the mechanism or the guiding quality of the compliant structure.

The wheels are designed with wheel parts that are positioned and bolted down on a carrier beam structure. Multifilament bands are clamped, roll off the wheel surfaces and connect the intermediate and final stages of the guiding mechanisms with the inner and outer wheel.

The modular design furthermore provides us with the opportunity to methodically investigate the effect of certain misalignments to the movement and hysteretic properties of the QEMMS mechanism. This helps to further clarify which design parameters matter not just from a theoretical, but from a practical point of view and highlights practical requirements to precision in assembling.

## Conclusion

In this article we discuss the requirements and design for a new mechanism for the Kibble balance in the Quantum Electro-Mechanical Metrology Suite (QEMMS) currently under construction at NIST. Summarizing the explanations on the previous pages, we designed a fully mechanical and flexure-based balance mechanism that can execute both modes of operation in the Kibble balance experiment—the weighing and the velocity mode. This mechanism constrains the trajectory of the moving components to a purely linear, one-dimensional motion by design without requiring auxiliary active control features.

Experiments regarding the guiding quality and repeatability of the mechanism will show the technological limitations of the flexure design. Due to the modular design, we can optimize the mechanism after evaluation of experimental results methodically piece by piece to converge to a design with the properties we desire for the QEMMS mechanism.

A prudent design is to theoretically minimize the known factors contributing to the hysteretic effect, such as the spring constant and loss factor. However, ambiguity remains about the contribution of mechanical hysteresis to the uncertainty budget.

## Availability of data and materials

Available on request.

## References

Kibble B. A measurement of the gyromagnetic ratio of the proton by the strong field method. In: Atomic masses and fundamental constants. vol. 5. 1976. p. 545–51.

The BIPM and the metre convention: The International System of Units (SI), 117–216 (2019)

Tiesinga E, Mohr P, Newell D, Taylor B. Codata recommended values of the fundamental physical constants. Rev Mod Phys. 2021;2018:93.

Delahaye F, Jeckelmann B. Revised technical guidelines for reliable dc measurements of the quantized Hall resistance. Metrologia. 2003;40:217–40.

Jeckelmann B, Jeanneret B. The quantum Hall effect as an electrical resistance standard. Rep Prog Phys. 2001;64:1603–58.

Hamilton C. Josephson voltage standards. Rev Sci Instrum. 2000;71:3611–26.

Haddad D, Seifert F, Chao L, Li S, Newell D, Pratt J, Williams C, Schlamminger S. Bridging classical and quantum mechanics. Metrologia. 2016;53:83–5.

Robinson I, Schlamminger S. The watt or Kibble balance: a technique for implementing the new SI definition of the unit of mass. Metrologia. 2016;53:46–74.

Kruskopf M, Pakdehi KDM, Pierz WS, Stosch R, Dziomba T, Götz M, Baringhaus J, Aprojanz J, Tegenkamp C, Lidzba J. Comeback of epitaxial graphene for electronics: large-area growth of bilayer-free graphene on sic. 2d materials. 2D Mater. 2016;3:041002.

Panna A, Hu I, Kruskopf M, Patel D, Jarrett D, Liu C, Payagala S, Saha D, Rigosi A, Newell D, Liang C, Elmquist R. Graphene quantum Hall effect parallel resistance arrays. Phys Rev B. 2021;103:075408.

Rigosi A, Panna A, Payagala S, Kruskopf M, Kraft M, Jones G, Wu B, Lee H, Yang Y, Hu J, Jarrett D, Newell D, Elmquist R. Graphene devices for tabletop and high-current quantized Hall resistance standards. IEEE Trans Instrum Meas. 2019;68:1870–8.

Marangoni R, Haddad D, Seifert F, Chao L, Newell D, Schlamminger S. Magnet system for the quantum electromechanical metrology suite. IEEE Trans Instrum Meas. 2020;69:5736–44.

Marangoni R, Haddad D, Seifert F, Chao L, Pratt J, Newell D, Schlamminger S. Design of the Kibble balance for the QEMMS. In: 2020 conference on precision electromagnetic measurements (CPEM). 2020. p. 1–2.

Darnieder M, Pabst M, Wenig R, Zentner L, Theska R, Fröhlich T. Static behavior of weighing cells. J Sens Sens Syst. 2018;2:587–600.

Darnieder M, Pabst M, Fröhlich T, Zentner L, Theska R. Mechanical properties of an adjustable weighing cell prototype. In: Euspen’s 19th international conference and exhibition. 2019.

Pratt J, Newell D, Kramar J. A flexure balance with adjustable restoring torque for nanonewton force measurement. In: International measurement confederation. 2002.

Sanchez C, Wood B, Green R, Liard J, Inglis D. A determination of Planck’s constant using the NRC watt balance. Metrologia. 2014;51:5–14.

Haddad D, Seifert F, Chao L, Li S, Newell D, Pratt J, Williams C, Schlamminger S. Invited article: a precise instrument to determine the Planck constant and the future kilogram. Rev Sci Instrum. 2016;87:061301.

Quinn T. The beam balance as an instrument for very precise weighing. Meas Sci Technol. 1992;3:141–59.

Speake C. Fundamental limits to mass comparison by means of a beam balance. Proc R Soc Lond Ser A, Math Phys Sci. 1987;414:333–58.

Speake C. Anelasticity in flexure strips revisited. Metrologia. 2018;55:114–9.

Rothleitner C, Schleichert J, Rogge N, Günther L, Vasilyan S, Hilbrunner F, Knopf D, Fröhlich T, Härtig F. The Planck–Balance—using a fixed value of the Planck constant to calibrate E1/E2-weights. Meas Sci Technol. 2018;29:074003.

Keck L, Shaw G, Theska R, Schlamminger S. Design of an electrostatic balance mechanism to measure optical power of 100 kW. IEEE Trans Instrum Meas. 2021;70:1–9.

Linß S. Ein Beitrag zur geometrischen Gestaltung und Optimierung prismatischer Festkörpergelenke in nachgiebigen Koppelmechanismen. PhD thesis, Technische Universiät Ilmenau, Fachgebiet Nachgiebige Systeme; 2015

Panas R, Hopkins J. Eliminating underconstraint in double parallelogram flexure mechanisms. J Mech Des. 2015;137:1–9.

Kibble B, Robinson I. Principles of a new generation of simplified and accurate watt balances. Metrologia. 2014;51:132–9.

Niebauer TM, Sasagawa GS, Fallel JE, Hilt R, Klopping E. A new generation of absolute gravimeters. Metrologia. 1995;32:159.

Gillespie G, Fujii K, Newell DB, Olsen PT, Picard OA, Steiner RL, Stenbakken GN, Williams ER. Alignment uncertainties of the NIST watt experiment. IEEE Trans Instrum Meas. 1997;46:605–8.

Kramar J, Newell D, Pratt J. NIST electrostatic force balance experiment. In: International measurement confederation. 2002.

Cosandier F, Eichenberger A, Baumann H, Jeckelmann B, Bonny M, Chatagny V, Clavel R. Development and integration of high straightness flexure guiding mechanisms dedicated to the METAS watt balance Mark II. Metrologia. 2014;51:88–95.

## Acknowledgements

The authors would like to thank Jon Pratt and Leon Chao from the Fundamental Electrical Measurements Group at NIST for valuable input and discussion during the design process.

## Funding

U.S. Government.

## Author information

### Authors and Affiliations

### Contributions

LK synthesized the concept, conducted analysis and designed the mechanism guided by FS and DH. SS, DN, and RT gave constant, valuable inputs regarding data analysis and practical aspects of the design and manufacturing. LK and DH were the major contributors in writing the manuscript. All authors read and approved the final manuscript.

### Corresponding authors

## Ethics declarations

### Competing interests

The authors declare that they have no competing interests.

## Appendices

### Appendix A

Here, we discuss three errors introduced to the measurement with the Kibble balance in the velocity mode stemming from imperfections in the motion of the coil from the vertical. We limit the explanations to the *x*-direction and linear assumptions for simplicity. The errors describe systematic biases, that we are estimating with an upper limit value. In reality, once we build the experiment, we will measure all the imperfection terms in situ, e.g., the wave front distortion, the beam diameter, the horizontal motion of the balance mechanism, …, and apply corrections for these biases.

### A.1 Voltage bias

Horizontal velocities also cause a bias \(e_{\mathrm{V}}\) in the readouts of the induced voltage in the velocity mode. This stems from both horizontal forces \(F_{\mathrm{x}}\) to the coil produced in the weighing mode—when the electrical center of the coil is not aligned with the magnetic center of the permanent magnet—and horizontal velocities in the velocity mode. The relative bias is expressed as follows

where \(F_{\mathrm{z}}\) is the force applied in the vertical direction by the magnet-coil system in weighing mode. The factor \(F_{\mathrm{x}}/F_{\mathrm{z}}\) is typically on the order of \(1\times 10^{-5}\) [17, 18], thus this bias yields \(e_{\mathrm{V}}={1.7\times 10^{-9}}\). However, this effect can be cancelled according to [26] when employing a balance mechanism that performs the exact same motion in the weighing and the velocity mode, which is the goal for the QEMMS mechanism.

### A.2 Beam shear bias

A contribution to a bias in the velocity mode is the beam shear error \(e_{\mathrm{BS}}\) in the interferometer. It occurs when the coil moves horizontal and the back-reflected interferometer beam gets displaced horizontally such that there is change in overlap between the reference beam and the beam reflected off of the moving retroreflector at the coil. The important values here are the wavelength of the laser, *λ*, the wave distortion at the optics—we assume \(\lambda /10\)—the beam shear/horizontal coil motion, Δ*x*, and the diameter of the laser beam in the interferometer, \(d_{\mathrm{Beam}}\). The equation for this relative bias derived from [27] is

The wavelength of the laser is \(\lambda = {633}~\mathrm{nm}\) with a beam diameter of \(d_{\mathrm{Beam}} = {6}~\mathrm{mm}\) which yields a bias of \(e_{\mathrm{BS}} = {3.52\times 10^{-9}}\).

### A.3 Velocity bias

Another measurement bias, \(e_{\mathrm{v}}\), comes from horizontal velocities during the velocity mode. These are derived from a misalignment of the interferometer with respect to gravity, *α*, and from the horizontal motion, Δ*x*, along the vertical coil travel Δ*z* [18, 28]. The equation for the bias is

Assuming a reasonable value \(\alpha = {45}~\upmu \text{{rad}}\), we get a relative measurement bias of \(e_{\mathrm{v}} = {7.5\times 10^{-9}}\), which is on the order of magnitude we desire to have.

### Appendix B

Figure 11 explains design principles to correct for motion imperfections in kinematic chains transitioning from a purely rotational to a purely translational motion of a moving member in a mechanism.

A purely rotational motion (1.) is turned into a quasi-linear motion of a plane with a systematic horizontal part (\(x'\)) through parallel setup of two beams as in a parallel four bar linkage (2.). Now we can use a serial (folded) chain of these linkages. By moving (\(z''\)) half the distance of (\(z'\)) we can correct for the parasitic horizontal part of the motion in the final stage. However, this is a movable system with two degrees of freedom, where the movement of the intermediate stage on the right (\(z''\)) is not coupled to the final stage on the left (\(z'\)) (3.). Furthermore, if the equation \(z'' = 2z'\) is not fulfilled here, there is going to be a certain \(x'\) in the final trajectory. In a final step, applying an external linkage (4.1) or parallel setup (4.2) we can constrain the motion to a single degree of freedom, as long as the condition \(z'' = 2z'\) is fulfilled by design.

Option (4.1) was used, e.g., as the mechanism in an electrostatic balance at NIST [29], and option (4.2) as the dedicated guiding mechanism for the Mark II Kibble balance of the Federal Institute of Metrology (METAS) of Switzerland [30].

### Appendix C

We derive the non-linear stiffness from the simplified model of a beam balance connected with a guiding mechanism on both sides in Fig. 12.

The horizontal force \(F_{\mathrm{H}}\) depending on the rotational deflection *φ* is described with

truncating the Taylor approximations for sine and cosine after the second order term.

The lever arm \(z' = l_{\mathrm{1}} \varphi \) introduces a moment \(M_{\mathrm{H}} (\varphi )\) through each side of the beam according to

which points out a third order dependency of the induced moment on the deflection angle *φ*.

For simplification, we assume that we compensate a constant, elastic part of the flexure stiffness in the mechanism entirely by using, e.g., an inverted pendulum. Building the derivative of the previous equation due to *φ* yields the non-linear rotational stiffness term induced by the parasitic horizontal force \(F_{\mathrm{H}}\)

Unfortunately, this term becomes highly dominant with larger deflections as can be seen in the upper plot in Fig. 13. With reasonable values for the system parameters shown in Fig. 12, a study at a simplified beam balance-based mechanism model using finite element analysis was conducted. Figure 14 shows the model and boundary conditions therefore.

The force over displacement curve of the final stage of the mechanism was monitored and compared to the analytical model. The rotational stiffness in equation (10) can be transferred to a linear stiffness at the guiding mechanism in vertical direction by dividing equation (10) by the square of the balance lever arm \(l_{\mathrm{1}}^{2}\). Furthermore, \(\varphi \approx \Delta z / l_{\mathrm{1}}\).

Note that the constant offset of the dashed from the solid green line in Fig. 13 stems from a residual constant stiffness part in the simulation model, which can, in practice, be compensated by adjusting the center of mass of the beam [16].

Furthermore, the horizontal force \(F_{\mathrm{H}}\) acting upon the flexure-based guiding mechanism affects the quality of guiding. The simulation yielding the results for the stiffness of the mechanism in Fig. 13 also provides insights to this horizontal trajectory error, d*x*, along the vertical displacement axis in *z*-direction displayed in the lower plot in Fig. 13. We see that the total horizontal error motion is approximately 20 times larger than allowed.

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## About this article

### Cite this article

Keck, L., Seifert, F., Newell, D. *et al.* Design of an enhanced mechanism for a new Kibble balance directly traceable to the quantum SI.
*EPJ Techn Instrum* **9**, 7 (2022). https://doi.org/10.1140/epjti/s40485-022-00080-3

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DOI: https://doi.org/10.1140/epjti/s40485-022-00080-3

### Keywords

- Kibble balance
- Mechanism
- Flexure
- Quantum SI